Rafidain Journal of Science

Current Issue

By Issue

By Subject

Keyword Index

Author Index

Indexing Databases XML

About Journal

Aims and Scope

Editorial Board

Facts and Figures

Publication Ethics

Indexing and Abstracting

Peer Review Process

News

Digital Archiving

Open Access Statement

Authorship

Appeals and complaints

Creative Commons Licence

Journal Funding Sources

Plagiarism Policy

Allegations of Misconduct

Copy Right Policies

The Identification and Synthesis of Barium-Substituted Lead Hydroxyapatite Structure (Pb10-x Bax (PO4)6(OH)2) by Ceramic Method

Rafidain Journal of Science, 2023, Volume 32, Issue 1, Pages 121-126
10.33899/rjs.2023.177294

Abstract

The substitution of barium ion (Ba2+) with lead ion (Pb2+) in the following composition: Pb10-x Bax (PO4)6(OH)2 has been investigated by an X-ray diffractometer. Samples with the range x=0 up to x=5 were calcined at 800 ºC for 25 hours, and the samples with the range from x=6 up to x=10 were calcined at 1100 ºC for 15 hours. The solid solutions hydroxyapatite samples are synthesized by the ceramic method. It was established that the sample with x=0 showed only reflections of composition Pb10(PO4)6(OH)2, while the sample with x=10 showed only reflections of composition Ba10(PO4)6(OH)2.The Samples with x = 1–9 showed more reflections called "unknown phase" besides those of pure hydroxyapatite.
 
Keywords:
Main Subjects:
  • Article View: 19
  • PDF Download: 21